2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

Base Information

Chemical Name:2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene
CAS No.:1240520-89-1
Molecular Formula:C₂₂H₃₃ClO
Molecular Weight:348.956
Hs Code.:

Synonyms:2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

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Chemical Property of 2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

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Technology Process of 2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

There total 2 articles about 2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1240520-88-0
(1R,3S,4R)-2,2-dichloro-4-methyl-3-((S)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl trifluoromethanesulfonate

: 1240520-89-1
2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/ol101559b

Reference yield: 93.0%

: 1240520-87-9
(1R,3S,4R)-2,2-dichloro-4-methyl-3-((S)-1-(2,4,6-triisopropylphenyl)ethoxy)cyclobutyl methanesulfonate

: 1240520-89-1
2-((S)-1-((1S,4S)-2-chloro-4-methylcyclobut-2-enyloxy)ethyl)-1,3,5-triisopropylbenzene

Guidance literature:: With zinc/copper couple; ammonium chloride; In methanol; diethyl ether; at 30 - 35 ℃; for 2.41667h; Inert atmosphere; Sonication;
DOI:10.1021/ol101559b