(3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

Base Information

Chemical Name:(3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester
CAS No.:81366-43-0
Molecular Formula:C₁₃H₁₅NO₆
Molecular Weight:281.265
Hs Code.:

Synonyms:(3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

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Chemical Property of (3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

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Technology Process of (3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

There total 13 articles about (3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 81366-42-9
(2S,3S)-2-Benzyloxycarbonylamino-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-hydroxy-propionic acid tert-butyl ester

: 81366-43-0
(3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

Guidance literature:: With water; trifluoroacetic acid; at 0 ℃; for 7h;
DOI:10.1246/cl.1982.145

Reference yield: 76.0%

: (2S,3S,4R)-2-Benzyloxycarbonylamino-3,4,5-trihydroxy-pentanoic acid methyl ester

: 81366-43-0
(3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

Guidance literature:: With silica gel;

Reference yield:

: 654083-18-8
(4S,5R)-[4-hydroxy-2-oxo-5-(tetrahydropyran-2-yloxymethyl)tetrahydrofuran-3-yl]carbamic acid benzyl ester

: 81366-48-5
(3R,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

: 81366-43-0
(3S,4S,5R)-(4-hydroxy-5-hydroxymethyl-2-oxotetrahydrofuran-3-yl)carbamic acid benzyl ester

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 50 ℃; for 10h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2003.10.005