N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

Base Information

Chemical Name:N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester
CAS No.:113490-71-4
Molecular Formula:C₂₁H₂₁NO₅S
Molecular Weight:399.467
Hs Code.:

Synonyms:N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

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Chemical Property of N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

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Technology Process of N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

There total 1 articles about N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 98-91-9
thiobenzoic acid

: 57653-38-0
N-<(phenylmethoxy)carbonyl>-4(R)-<<(4-methylphenyl)sulfonyl>oxy>-(S)-proline methyl ester

: 113490-71-4
N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; for 44h; Heating;
DOI:10.1021/jm00399a033

Reference yield: 87.0%

: 113490-71-4
N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

: (2S,4S)-4-Benzoylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester; hydrobromide

Guidance literature:: With hydrogen bromide; acetic acid; for 2h; Ambient temperature;
DOI:10.1021/jm00399a033

Reference yield:

: 113490-71-4
N-<(phenylmethoxy)carbonyl>-4(S)-(benzoylthio)-(S)-proline methyl ester

: (2S,4S)-1-(3-Acetylsulfanyl-2-methyl-propionyl)-4-benzoylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HBr, HOAc / 2 h / Ambient temperature

2: 90 percent / pyridine / 18 h / Ambient temperature

With hydrogen bromide; acetic acid; In pyridine;
DOI:10.1021/jm00399a033