(E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate

Base Information

Chemical Name:(E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate
CAS No.:1030604-10-4
Molecular Formula:C₂₄H₃₆O₄Si
Molecular Weight:416.633
Hs Code.:

Synonyms:(E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate

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Chemical Property of (E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate

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Technology Process of (E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate

There total 1 articles about (E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1030604-04-6
((R)-1-(benzyloxy)-2-((R,z)-2-vinylcyclohept-2-enyl)propan-2-yloxy)trimethylsilane

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1030604-10-4
(E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 40 ℃; for 42h; Inert atmosphere;
DOI:10.1021/ol800418m

Reference yield:

: 1030604-10-4
(E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate

: C₂₄H₃₈O₆Si

Guidance literature:: (E)-methyl 3-((R,Z)-7-((R)-1-(benzyloxy)-2-(trimethylsilyloxy)propan-2-yl)cyclohept-1-enyl)-acrylate; With potassium osmate; methanesulfonamide; (DHQ)2PHAL; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 4h; Inert atmosphere;

With sodium sulfite; In water; tert-butyl alcohol; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol800418m