2-Amino-1-(3-chloro-4-hydroxyphenyl)ethanone

Base Information

• Chemical Name: 2-Amino-1-(3-chloro-4-hydroxyphenyl)ethanone
• CAS No.: 73898-70-1
• Molecular Formula: C₈H₈ClNO₂
• Molecular Weight: 185.61
• DSSTox Substance ID: DTXSID801255509

Synonyms:2-amino-1-(3-chloro-4-hydroxyphenyl)ethanone;73898-70-1;DTXSID801255509;EN300-1984781;2-amino-1-(3-chloro-4-hydroxyphenyl)ethan-1-one

Chemical Property of 2-Amino-1-(3-chloro-4-hydroxyphenyl)ethanone

Chemical Property:

• XLogP3: 1.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 185.0243562
• Heavy Atom Count: 12
• Complexity: 174

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=C(C=C1C(=O)CN)Cl)O

Technology Process of 2-Amino-1-(3-chloro-4-hydroxyphenyl)ethanone

There total 1 articles about 2-Amino-1-(3-chloro-4-hydroxyphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-Butyl nitrite (544-16-1) → 2-amino-1-(3-chloro-4-hydroxyphenyl)ethyl ketone (73898-70-1)

Guidance literature:

With hydrogenchloride; diethyl ether; anschliessends Behandeln mit Zinn(II)-chlorid;

Reference yield:

gemfibrozil (25812-30-0) + 2-amino-1-(3-chloro-4-hydroxyphenyl)ethyl ketone (73898-70-1) → C23H29ClN2O3 (1416548-85-0)

Guidance literature:

gemfibrozil; 2-amino-1-(3-chloro-4-hydroxyphenyl)ethyl ketone; With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h;

With ammonia; for 0.5h; Reflux;

upstream raw materials:

n-Butyl nitrite

Downstream raw materials:

C₂₃H₂₉ClN₂O₃

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