C₂₉H₄₄O₆Si

Base Information

Chemical Name:C₂₉H₄₄O₆Si
CAS No.:1350544-19-2
Molecular Formula:C₂₉H₄₄O₆Si
Molecular Weight:516.75
Hs Code.:

C<sub>29</sub>H<sub>44</sub>O<sub>6</sub>Si

Synonyms:C₂₉H₄₄O₆Si

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Chemical Property of C₂₉H₄₄O₆Si

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Technology Process of C₂₉H₄₄O₆Si

There total 10 articles about C₂₉H₄₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1350544-18-1
C₂₉H₄₆O₆Si

: 1350544-19-2
C₂₉H₄₄O₆Si

Guidance literature:: C₂₉H₄₆O₆Si; With oxalyl dichloride; In dichloromethane; dimethyl sulfoxide; at -78 ℃; for 4h; Inert atmosphere;

With triethylamine; In dichloromethane; dimethyl sulfoxide; at -78 - 0 ℃; for 0.583333h; Inert atmosphere;
DOI:10.1021/ol202728v

Reference yield:

: 1350544-09-0
C₂₄H₃₆O₅Si

: 1350544-19-2
C₂₉H₄₄O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: titanium tetrachloride / toluene / 1.17 h / -78 °C / Inert atmosphere

1.2: 3.5 h / -78 - 5 °C

2.1: 1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide / acetonitrile / 3 h / 82 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 3 h / 23 °C / Inert atmosphere

4.1: diethylzinc / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

4.2: 0.67 h / -78 - 0 °C / Inert atmosphere

4.3: 0.42 h / -78 - -20 °C / Inert atmosphere

5.1: cerium(III) chloride; lithium chloride / diethyl ether / 3.25 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 - 0 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / benzene / 4.5 h / 23 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 7 h / -78 - -5 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

9.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / 4 h / -78 °C / Inert atmosphere

9.2: 0.58 h / -78 - 0 °C / Inert atmosphere

With cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; diethylzinc; pyridinium p-toluenesulfonate; titanium tetrachloride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile; benzene; 1.1: Diels-Alder reaction / 1.2: Diels-Alder reaction / 9.1: Swern oxidation / 9.2: Swern oxidation;
DOI:10.1021/ol202728v

Reference yield:

: 1350544-10-3
C₂₈H₄₂O₅Si

: 1350544-19-2
C₂₉H₄₄O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1,1,1,3,3,3-hexamethyl-disilazane; sodium iodide / acetonitrile / 3 h / 82 °C / Inert atmosphere

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 3 h / 23 °C / Inert atmosphere

3.1: diethylzinc / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

3.2: 0.67 h / -78 - 0 °C / Inert atmosphere

3.3: 0.42 h / -78 - -20 °C / Inert atmosphere

4.1: cerium(III) chloride; lithium chloride / diethyl ether / 3.25 h / -78 °C / Inert atmosphere

4.2: 2 h / -78 - 0 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / benzene / 4.5 h / 23 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 7 h / -78 - -5 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

8.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / 4 h / -78 °C / Inert atmosphere

8.2: 0.58 h / -78 - 0 °C / Inert atmosphere

With cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; diethylzinc; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile; benzene; 8.1: Swern oxidation / 8.2: Swern oxidation;
DOI:10.1021/ol202728v