1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

Base Information

Chemical Name:1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide
CAS No.:1445981-49-6
Molecular Formula:C₁₉H₁₉Cl₂NO₃
Molecular Weight:380.271
Hs Code.:

Synonyms:1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

Chemical Property:

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Technology Process of 1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

There total 4 articles about 1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1445984-98-4
1-(2,5-dichlorobenzyloxy)cyclopropanecarboxylic acid

: 10541-78-3
2-methoxy-N-methylaniline

: 1445981-49-6
1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In acetonitrile; at 20 ℃; for 24h;

Reference yield:

: 2745-49-5
1,4-Dichloro-2-chloromethyl-benzene

: 1445981-49-6
1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diazomethyl-trimethyl-silane / methanol; diethyl ether; dichloromethane / 0.17 h / 20 °C

1.2: 0.08 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 24 h / 20 °C

With N-ethyl-N,N-diisopropylamine; HATU; diazomethyl-trimethyl-silane; In methanol; diethyl ether; dichloromethane; acetonitrile;

Reference yield:

: 1445985-43-2
methyl 1-[(2,5-dichlorophenyl)methoxy]cyclopropane-1-carboxylate

: 1445981-49-6
1-(2,5-dichlorobenzyloxy)-N-(2-methoxyphenyl)-N-methylcyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide / tetrahydrofuran / 30 °C

2: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 24 h / 20 °C

With water; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In tetrahydrofuran; acetonitrile;