methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside
CAS No.:158975-62-3
Molecular Formula:C₃₁H₃₅NO₈
Molecular Weight:549.621
Hs Code.:

methyl 3,4,6-tri-O-benzyl-2-C-<N-(carboxymethyl)carbamoyl>-2-deoxy-β-D-glucopyranoside

Synonyms:methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

There total 2 articles about methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158975-58-7
methyl 3,4,6-tri-O-benzyl-2-C-(N-tert-butoxycarbonylmethylcarbamoyl)-2-deoxy-β-D-glucopyranoside

: 158975-62-3
methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 1.5h; Ambient temperature;
DOI:10.1016/0008-6215(94)84216-7

Reference yield:

: 135735-81-8
methyl 3,4,6-tri-O-benzyl-2-deoxy-2-C-(tosylcarbamoyl)-β-D-glucopyranoside

: 158975-62-3
methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / KOH, Bu₄NBr / benzene / 4 h / Ambient temperature

2: 70 percent / sodium naphthalenide / 1,2-dimethoxy-ethane / 0.33 h / -30 °C

3: TFA / CH₂Cl₂ / 1.5 h / Ambient temperature

With potassium hydroxide; tetrabutylammomium bromide; sodium naphthalenide; trifluoroacetic acid; In 1,2-dimethoxyethane; dichloromethane; benzene;
DOI:10.1016/0008-6215(94)84216-7

Reference yield: 67.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 158975-62-3
methyl 3,4,6-tri-O-benzyl-2-C--2-deoxy-β-D-glucopyranoside

: 158975-64-5
N-<(methyl 3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosid-2-yl)carbonyl>glycylglycine methyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(94)84216-7