diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

Base Information

Chemical Name:diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside
CAS No.:335591-72-5
Molecular Formula:C₉₇H₁₁₂O₂₄
Molecular Weight:1661.94
Hs Code.:

Synonyms:diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

There total 5 articles about diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (Z)-5-(2'-hexynylphenyl)-4-pentenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside

: 335591-63-4
diosgen-3-yl 3,6-di-O-pivaloyl-β-D-glucopyranoside

: 335591-72-5
diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

Guidance literature:: With mercury di[bis(trifluoromethylsulfonyl)imide]; In dichloromethane; at 20 ℃; for 5.5h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b03038

Reference yield: 79.0%

: 151767-11-2
2,3,4,5-tetra-O-benzoyl-D-glucopyranosyl trichloroacetimidate

: 335591-63-4
diosgen-3-yl 3,6-di-O-pivaloyl-β-D-glucopyranoside

: 335591-72-5
diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1246/cl.2012.1015

Reference yield: 60.0%

: 14218-08-7,41881-44-1,53297-33-9,60820-93-1,61198-82-1,67986-91-8,73068-86-7,131897-72-8,131897-73-9
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl bromide

: 335591-63-4
diosgen-3-yl 3,6-di-O-pivaloyl-β-D-glucopyranoside

: 335591-64-5
diosgenyl 2,3,4-tri-O-benzoyl-α–L-rhamnopyranosyl-(1→2)-3,6-di-O-pivaloyl-β-D-glucopyranoside

: 335591-72-5
diosgenyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→4)-[2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)]-3,6-di-O-pivaloyl-β-D-glucopyranoside

Guidance literature:: With 4 Angstroem MS; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -16 ℃; for 2h;
DOI:10.1016/S0008-6215(01)00014-3