C₆₀H₁₁₀O₁₂Si₃

Base Information

Chemical Name:C₆₀H₁₁₀O₁₂Si₃
CAS No.:866021-57-0
Molecular Formula:C₆₀H₁₁₀O₁₂Si₃
Molecular Weight:1107.78
Hs Code.:

C<sub>60</sub>H<sub>110</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₆₀H₁₁₀O₁₂Si₃

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Chemical Property of C₆₀H₁₁₀O₁₂Si₃

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Technology Process of C₆₀H₁₁₀O₁₂Si₃

There total 31 articles about C₆₀H₁₁₀O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 866022-15-3
C₆₀H₁₀₈O₁₂Si₃

: 866021-57-0
C₆₀H₁₁₀O₁₂Si₃

Guidance literature:: With quinoline; hydrogen; Lindlar's catalyst; In ethanol;
DOI:10.1021/ol051405x

Reference yield:

: 866021-71-8
(4S,5S)-5-((S)-1-methoxybut-3-enyl)-2,2-dimethyl-1,3-dioxolane-4-carbaldehyde

: 866021-57-0
C₆₀H₁₁₀O₁₂Si₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: c-Hex₂BCl; Et₃N / diethyl ether / 0 °C

1.2: -78 °C

1.3: 79 percent / aq. H₂O₂

2.1: 2,6-lutidine / CH₂Cl₂

3.1: K₂CO₃ / methanol

4.1: NaBH₄

5.1: NaIO₄

6.1: NaBH₄

7.1: PPTS / CH₂Cl₂

8.1: tetrahydrofuran

9.1: aq. H₂O₂; NaOH

10.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂

11.1: n-BuLi / tetrahydrofuran / -78 °C

12.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂

13.1: H₂; quinoline / Pd/CaCO₃/Pb / ethanol

With 2,6-dimethylpyridine; quinoline; sodium hydroxide; sodium tetrahydroborate; sodium periodate; n-butyllithium; dicyclohexylboron chloride; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; triethylamine; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; 10.1: Dess-Martin oxidation / 12.1: Dess-Martin oxidation / 13.1: Lindlar hydrogenation;
DOI:10.1021/ol051405x

Reference yield:

: 866021-62-7
((2R,6S)-6-allyltetrahydropyran-2-yl)acetic acid ethyl ester

: 866021-57-0
C₆₀H₁₁₀O₁₂Si₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: O₃ / CH₂Cl₂ / -78 °C

1.2: PPh₃ / CH₂Cl₂

2.1: diethyl ether / -78 °C

3.1: LiAlH₄ / diethyl ether / -78 °C

4.1: imidazole; DMAP / dimethylformamide

5.1: O₃ / CH₂Cl₂ / -78 °C

5.2: PPh₃ / CH₂Cl₂

6.1: (-)-Ipc₂BCl; Et₃N / diethyl ether / -78 °C

6.3: 87 percent / aq. H₂O₂; pH 7 buffer / methanol / pH 7

7.1: Me₄NBH(OAc)3; AcOH / acetonitrile / -30 °C

8.1: PPTS

9.1: H₂ / Pd(OH)2-C / ethyl acetate

10.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂

11.1: PPh₃; Et₃N / CH₂Cl₂ / 0 °C

12.1: n-BuLi / tetrahydrofuran / -78 °C

13.1: n-BuLi / tetrahydrofuran / -78 °C

14.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂

15.1: H₂; quinoline / Pd/CaCO₃/Pb / ethanol

With 1H-imidazole; quinoline; dmap; lithium aluminium tetrahydride; n-butyllithium; hydrogen; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; ozone; acetic acid; triethylamine; triphenylphosphine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride; Lindlar's catalyst; palladium hydroxide - carbon; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 10.1: Dess-Martin oxidation / 14.1: Dess-Martin oxidation / 15.1: Lindlar hydrogenation;
DOI:10.1021/ol051405x