3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

Base Information

Chemical Name:3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide
CAS No.:948040-47-9
Molecular Formula:C₂₂H₂₃NO₈S₂
Molecular Weight:493.559
Hs Code.:

Synonyms:3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

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Chemical Property of 3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

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Technology Process of 3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

There total 5 articles about 3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 948040-46-8
3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptononitrile

: 948040-47-9
3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

Guidance literature:: With pyridine; hydrogen sulfide; at 20 ℃; for 336h;
DOI:10.1016/j.bmcl.2007.05.050

Reference yield:

: C₂₁H₂₀O₉S

: 948040-47-9
3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / methanol / 1.33 h / 0 - 20 °C

2: pyridine / CH₂Cl₂ / 1 h / -10 - 20 °C

3: 73 percent / dimethylformamide / 1.5 h / 20 °C

4: 78 percent / hydrogen sulfide; pyridine / 336 h / 20 °C

With pyridine; sodium tetrahydroborate; hydrogen sulfide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.05.050

Reference yield:

: 948040-44-6
2,5-anhydro-4,6-di-O-benzoyl-3-O-methanesulfonyl-D-glucitol

: 948040-47-9
3,6-anhydro-5,7-di-O-benzoyl-2-deoxy-4-O-methanesulfonyl-D-glucoheptonthioamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 1 h / -10 - 20 °C

2: 73 percent / dimethylformamide / 1.5 h / 20 °C

3: 78 percent / hydrogen sulfide; pyridine / 336 h / 20 °C

With pyridine; hydrogen sulfide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.05.050