4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

Base Information

Chemical Name:4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide
CAS No.:1351088-05-5
Molecular Formula:C₁₇H₂₃N₇O₃S
Molecular Weight:405.481
Hs Code.:

Synonyms:4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

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Technology Process of 4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

There total 5 articles about 4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1285113-52-1
3-amino-4-{ethyl[2-(methyloxy)ethyl]amino}-N-methylbenzenesulfonamide

: 87-42-3
6-chloropurine

: 1351088-05-5
4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

Guidance literature:: With silver trifluoromethanesulfonate; In 1,4-dioxane; at 100 ℃; for 20h; Microwave irradiation; Sealed tube;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1351088-05-5
4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: chlorosulfonic acid / 18 h / 100 °C

2: triethylamine / tetrahydrofuran / 1 h / -35 °C

3: 18 h / 110 °C / Sealed tube; Microwave irradiation

4: hydrogen / palladium on activated charcoal / ethanol / 1 h / 20 °C / 1810.07 Torr

5: silver trifluoromethanesulfonate / 1,4-dioxane / 20 h / 100 °C / Microwave irradiation; Sealed tube

With chlorosulfonic acid; hydrogen; silver trifluoromethanesulfonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol;

Reference yield:

: 6668-56-0
4-fluoro-3-nitrobenzene-1-sulfonyl chloride

: 1351088-05-5
4-{ethyl[2-(methyloxy)ethyl]amino}-N-methyl-3-(1H-purin-6-ylamino)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 1 h / -35 °C

2: 18 h / 110 °C / Sealed tube; Microwave irradiation

3: hydrogen / palladium on activated charcoal / ethanol / 1 h / 20 °C / 1810.07 Torr

4: silver trifluoromethanesulfonate / 1,4-dioxane / 20 h / 100 °C / Microwave irradiation; Sealed tube

With hydrogen; silver trifluoromethanesulfonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol;