C₃₀H₃₄NO₅P

Base Information

• Chemical Name: C₃₀H₃₄NO₅P
• CAS No.: 162306-34-5
• Molecular Formula: C₃₀H₃₄NO₅P
• Molecular Weight: 519.577
• Mol file: 162306-34-5.mol

Synonyms:C₃₀H₃₄NO₅P

Chemical Property of C₃₀H₃₄NO₅P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₄NO₅P

There total 2 articles about C₃₀H₃₄NO₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-azido-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose (21870-78-0) + triphenylphosphine (603-35-0) → C30H34NO5P (162306-34-5)

Guidance literature:

Staudinger reduction;

DOI:10.1021/jo00098a014

Reference yield:

1,2:5,6-di-O-isopropylidene-3-O-triflyl-α-D-glucofuranose (55951-93-4) → C30H34NO5P (162306-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NaN₃

2: Staudinger reduction

With sodium azide;

DOI:10.1021/jo00098a014

Reference yield:

C30H34NO5P (162306-34-5) → N-(1,2-O-isopropylidene-3-deoxy-α-D-allos-3-yl)-N-(methyl 5-deoxy-β-D-ribofuranoside-5-yl)amine (1430418-31-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 0.5 h / 0 °C / Inert atmosphere

2.1: sodium methylate / methanol / 20 °C

3.1: acetic acid / water / 45 °C

With sodium methylate; acetic acid; In tetrahydrofuran; methanol; water;

DOI:10.1016/j.carres.2013.02.002

upstream raw materials:

3-azido-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

triphenylphosphine

1,2:5,6-di-O-isopropylidene-3-O-triflyl-α-D-glucofuranose

Downstream raw materials:

N-(1,2-O-isopropylidene-3-deoxy-α-D-allos-3-yl)-N-(methyl 5-deoxy-β-D-ribofuranoside-5-yl)amine