C₂₆H₂₅NO₆

Base Information

• Chemical Name: C₂₆H₂₅NO₆
• CAS No.: 936572-48-4
• Molecular Formula: C₂₆H₂₅NO₆
• Molecular Weight: 447.488
• Mol file: 936572-48-4.mol

Synonyms:C₂₆H₂₅NO₆

Chemical Property of C₂₆H₂₅NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₅NO₆

There total 1 articles about C₂₆H₂₅NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

methyl 2-(benzyloxycarbonylamino)acrylate (21149-17-7) + (5-(benzyloxy)-2-iodophenyl)methanol (50765-13-4) → C26H25NO6 + C26H25NO6 (936572-48-4)

Guidance literature:

With tetrabutyl-ammonium chloride; triethylamine; palladium diacetate; In tetrahydrofuran; at 70 ℃; for 2.5h;

DOI:10.1016/j.tetlet.2007.02.078

Reference yield:

C26H25NO6 (936572-48-4) → C26H26ClNO5 (936572-58-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 95 percent / hydrogen; (+)-1,2-bis((2R,5R)-2,5-Et₂phospholano)Ph(c-octadiene)Rh*BF₄ / CH₂Cl₂; methanol

2: 99 percent / magnesium methoxide / CHCl₃; methanol

3: 86 percent / thionyl chloride / CH₂Cl₂

With thionyl chloride; hydrogen; magnesium methanolate; In methanol; dichloromethane; chloroform;

DOI:10.1016/j.tetlet.2007.02.078

Reference yield:

C26H25NO6 (936572-48-4) → C30H34N2O4 (936572-59-7)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 95 percent / hydrogen; (+)-1,2-bis((2S,5S)-2,5-Et₂phospholano)Ph(c-octadiene)Rh*BF₄ / CH₂Cl₂

2.1: 99 percent / magnesium methoxide / CHCl₃; methanol

3.1: 86 percent / thionyl chloride / CH₂Cl₂

4.1: CH₂Cl₂ / 24 h / 20 °C

4.2: 91 percent / aq. acetic acid / toluene; CH₂Cl₂ / Heating

With thionyl chloride; hydrogen; magnesium methanolate; In methanol; dichloromethane; chloroform;

DOI:10.1016/j.tetlet.2007.02.078

upstream raw materials:

methyl 2-(benzyloxycarbonylamino)acrylate

(5-(benzyloxy)-2-iodophenyl)methanol

Downstream raw materials:

C₂₈H₂₇NO₇

C₂₈H₂₉NO₇

C₂₆H₂₇NO₆

C₂₆H₂₆ClNO₅