N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

Base Information

Chemical Name:N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid
CAS No.:1415221-83-8
Molecular Formula:C₃₅H₃₉N₃O₄
Molecular Weight:565.712
Hs Code.:

Synonyms:N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

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Chemical Property of N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

Chemical Property:

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Technology Process of N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

There total 4 articles about N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₉N₃O₂

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1415221-83-8
N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2012.10.093

Reference yield:

: 10472-97-6
8-phenyloctan-1-ol

: 1415221-83-8
N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / -75 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / -75 - 20 °C / Inert atmosphere

3: hydrogenchloride / 24 h / Reflux

4: sodium hydrogencarbonate / 1,4-dioxane; water / 12 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.10.093

Reference yield:

: C₁₅H₂₁F₃O₃S

: 1415221-83-8
N--Fmoc--(2S)--2--amino--3--(1--(8--phenyloctyl)--1H--imidazol--4--yl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / -75 - 20 °C / Inert atmosphere

2: hydrogenchloride / 24 h / Reflux

3: sodium hydrogencarbonate / 1,4-dioxane; water / 12 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.10.093