<6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

Base Information

Chemical Name:<6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester
CAS No.:143488-23-7
Molecular Formula:C₂₉H₂₅IN₂O₅S
Molecular Weight:640.498
Hs Code.:

Synonyms:<6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

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Chemical Property of <6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

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Technology Process of <6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

There total 3 articles about <6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 143488-22-6
<6R-<6α,7β(R)>>-3-(chloromethyl)-7-<(hydroxyphenylacetyl)amino>-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenylmethyl ester

: 143488-23-7
<6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

Guidance literature:: With sodium iodide; In butanone; for 2h; Ambient temperature;

Reference yield:

: 611-71-2
(R)-Mandelic Acid

: 143488-23-7
<6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 1-hydroxybenzotriazole, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂

2: 93 percent / NaI / butan-2-one / 2 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium iodide; In dichloromethane; butanone;

Reference yield:

: (6R)-trans-3-chloromethyl-7-amino-8-oxo-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylate, diphenylmethyl ester

: 143488-23-7
<6R-<6α,7β(R)>>-7-<(hydroxyphenylacetyl)amino>-3-(iodomethyl)-8-oxo-5-thia-1-azabicyclo<4.2.0>oct-2-ene-2-carboxylic acid diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 1-hydroxybenzotriazole, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂

2: 93 percent / NaI / butan-2-one / 2 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium iodide; In dichloromethane; butanone;