C₂₃H₂₄N₂O₆S

Base Information

Chemical Name:C₂₃H₂₄N₂O₆S
CAS No.:1093120-82-1
Molecular Formula:C₂₃H₂₄N₂O₆S
Molecular Weight:456.519
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:C₂₃H₂₄N₂O₆S

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Chemical Property of C₂₃H₂₄N₂O₆S

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Technology Process of C₂₃H₂₄N₂O₆S

There total 5 articles about C₂₃H₂₄N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1093121-29-9
C₂₄H₂₆N₂O₆S

: 1093120-82-1
C₂₃H₂₄N₂O₆S

Guidance literature:: C₂₄H₂₆N₂O₆S; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 24h;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate; pH=2;

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1093120-82-1
C₂₃H₂₄N₂O₆S

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / acetonitrile / 12 h / 85 °C / Heating / reflux

2.1: lithium hydroxide; water / tetrahydrofuran / 12 h / 45 °C

2.2: pH 2

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 20 °C

4.1: lithium hydroxide; water / tetrahydrofuran / 24 h / 20 °C

4.2: pH 2

With lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; water; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 19438-10-9
methyl 3-hydroxybenzoate

: 1093120-82-1
C₂₃H₂₄N₂O₆S

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / acetone / 15 h / 20 - 55 °C

2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 20 °C

3.1: lithium hydroxide; water / tetrahydrofuran / 24 h / 20 °C

3.2: pH 2

With lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; water; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;