[Ir(1-(4,6-difluorophenyl)-pyrazolato-C₂,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate

Base Information

• Chemical Name: [Ir(1-(4,6-difluorophenyl)-pyrazolato-C₂,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate
• CAS No.: 1015446-32-8
• Molecular Formula: C₄₃H₃₀F₄IrN₆O₂*F₆P
• Molecular Weight: 1075.93

Synonyms:[Ir(1-(4,6-difluorophenyl)-pyrazolato-C₂,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate

Chemical Property of [Ir(1-(4,6-difluorophenyl)-pyrazolato-C₂,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate

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Technology Process of [Ir(1-(4,6-difluorophenyl)-pyrazolato-C₂,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate

There total 1 articles about [Ir(1-(4,6-difluorophenyl)-pyrazolato-C₂,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

ammonium hexafluorophosphate + bis-(μ)-chlorotetrakis(1-(4,6-difluorophenyl)-pyrazolato-C2,N)diiridium(III) (562099-13-2) + 9,9-bis(4-methoxyphenyl)-9H-4,5-diazafluorene (686342-56-3) → [Ir(1-(4,6-difluorophenyl)-pyrazolato-C2,N)2(9,9-bis(4-methoxyphenyl)-4,5-diazafluorene)]hexafluorophosphate (1015446-32-8)

Guidance literature:

In ethylene glycol; (Ar); heating soln. of iridium compd. and diazafluorene deriv. in ethylene glycol at 150°C for 16 h, cooling o room temp., addn. of aq. soln. of NH4PF6; filtration, drying in oven at 80°C for 12 h, chromy. (silica gel,CH2Cl2/CH3CN (10:1)), NMR and HRMS;

DOI:10.1021/ja076051e

upstream raw materials:

bis-(μ)-chlorotetrakis(1-(4,6-difluorophenyl)-pyrazolato-C²,N)diiridium(III)

9,9-bis(4-methoxyphenyl)-9H-4,5-diazafluorene

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