Technology Process of C28H20Cl2N2O4
There total 3 articles about C28H20Cl2N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; copper diacetate;
In
1,2-dichloro-ethane;
at 20 ℃;
for 24h;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride; hydrazine hydrate / 1,4-dioxane; methanol / Reflux
2: pyridine; copper diacetate / 1,2-dichloro-ethane / 24 h / 20 °C / Molecular sieve
With
pyridine; hydrogenchloride; copper diacetate; hydrazine hydrate;
In
1,4-dioxane; methanol; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C
2: 1.42 h / 170 - 175 °C / microwave
3: hydrogenchloride; hydrazine hydrate / 1,4-dioxane; methanol / Reflux
4: pyridine; copper diacetate / 1,2-dichloro-ethane / 24 h / 20 °C / Molecular sieve
With
pyridine; hydrogenchloride; copper diacetate; potassium carbonate; hydrazine hydrate;
In
1,4-dioxane; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;