DIETHYL 2-(ACETYLAMINO)-2-[4-(METHOXYCARBONYL)BENZYL]MALONATE

Base Information

• Chemical Name: DIETHYL 2-(ACETYLAMINO)-2-[4-(METHOXYCARBONYL)BENZYL]MALONATE
• CAS No.: 109564-46-7
• Molecular Formula: C₁₈H₂₃NO₇
• Molecular Weight: 365.383
• Mol file: 109564-46-7.mol

Synonyms:diethyl (N-acetylamino)[{4-(methoxycarbonyl)phenyl}methyl]malonate

Chemical Property of DIETHYL 2-(ACETYLAMINO)-2-[4-(METHOXYCARBONYL)BENZYL]MALONATE

Chemical Property:

Purity/Quality:

Diethyl 2-(acetylamino)-2-[4-(methoxycarbonyl)benzyl]malonate ^*data from reagent suppliers

Safty Information:

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Technology Process of DIETHYL 2-(ACETYLAMINO)-2-[4-(METHOXYCARBONYL)BENZYL]MALONATE

There total 2 articles about DIETHYL 2-(ACETYLAMINO)-2-[4-(METHOXYCARBONYL)BENZYL]MALONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-acetylaminomalonic acid diethyl ester (1068-90-2) + [4-(methoxycarbonyl)phenyl]methyl methyl carbonate → diethyl (N-acetylamino)[{4-(methoxycarbonyl)phenyl}methyl]malonate (109564-46-7)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; 1,5-cis,cis-cyclooctadiene; [PdCp(η3-C3H5)]; In tetrahydrofuran; at 80 ℃;

DOI:10.1021/ol048540e

Reference yield:

→ diethyl (N-acetylamino)[{4-(methoxycarbonyl)phenyl}methyl]malonate (109564-46-7)

Guidance literature:

Na-acetamino-malonsaeure-diethylester, 4-Brommethyl-benzoesaeure-methylester in EtOH, (70-75grad);

upstream raw materials:

2-acetylaminomalonic acid diethyl ester

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