2-cyano-2-diazo-N,N-diphenethylacetamide

Base Information

Chemical Name:2-cyano-2-diazo-N,N-diphenethylacetamide
CAS No.:1431791-50-2
Molecular Formula:C₁₉H₁₈N₄O
Molecular Weight:318.378
Hs Code.:

Synonyms:2-cyano-2-diazo-N,N-diphenethylacetamide

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Chemical Property of 2-cyano-2-diazo-N,N-diphenethylacetamide

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Technology Process of 2-cyano-2-diazo-N,N-diphenethylacetamide

There total 2 articles about 2-cyano-2-diazo-N,N-diphenethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1431792-06-1
2-cyano-N,N-diphenethylacetamide

: 1431791-50-2
2-cyano-2-diazo-N,N-diphenethylacetamide

Guidance literature:: With 2,4,6-trimethyl-pyridine; imidazole-1-sulfonyl azide hydrochloride; In acetonitrile; at 55 ℃; for 24h; Sealed tube;
DOI:10.1021/ja401610p

Reference yield:

: 6308-98-1
diphenethylamine

: 1431791-50-2
2-cyano-2-diazo-N,N-diphenethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.67 h / 165 °C / Inert atmosphere; Microwave irradiation

2: imidazole-1-sulfonyl azide hydrochloride; 2,4,6-trimethyl-pyridine / acetonitrile / 24 h / 55 °C / Sealed tube

With 2,4,6-trimethyl-pyridine; imidazole-1-sulfonyl azide hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ja401610p

Reference yield: 93.0%

: 1431791-50-2
2-cyano-2-diazo-N,N-diphenethylacetamide

: C₁₉H₁₈N₂O

Guidance literature:: With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; In dichloromethane; 1,2-dichloro-ethane; at -40 - 22 ℃; Glovebox; Inert atmosphere;
DOI:10.1021/ja401610p