[(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-)

Base Information

Chemical Name:[(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-)
CAS No.:1016971-10-0
Molecular Formula:C₃₀H₃₅N₂Pd*F₆P
Molecular Weight:675.005
Hs Code.:

Synonyms:[(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-)

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Chemical Property of [(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-)

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Technology Process of [(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-)

There total 1 articles about [(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1016971-03-1
CH₃CN(C₆H₃(CH₃)2)CHCC₆H₅NH(C₆H₃(CH₃)2)

: methallyloxytris(dimethylamino)phosphonium hexafluorophosphate

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 1016971-10-0
[(2,6-(CH3)2-C6H3NC(Ph)CH2C(Me)NC6H3-2,6-(CH3)2)Pd(η3-C4H7)](1+)PF6(1-)

Guidance literature:: In dichloromethane; (Ar); equimolar Pd-compound dissolved in CH2Cl2; equimolar P-ligand and amine ligand added; stirred for 24 h at room temp.; sepd. by filtration through celite; solvent removed in vacuum; washed with Et2O 3 times; dried in vacuum; crystallized from CH2Cl2/n-hexane 1:1 mixt.; elem. anal.;
DOI:10.1016/j.poly.2007.11.026