C₂₂H₁₆F₃N₅O₂S

Base Information

Chemical Name:C₂₂H₁₆F₃N₅O₂S
CAS No.:1609271-86-4
Molecular Formula:C₂₂H₁₆F₃N₅O₂S
Molecular Weight:471.463
Hs Code.:

C<sub>22</sub>H<sub>16</sub>F<sub>3</sub>N<sub>5</sub>O<sub>2</sub>S

Synonyms:C₂₂H₁₆F₃N₅O₂S

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Chemical Property of C₂₂H₁₆F₃N₅O₂S

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Technology Process of C₂₂H₁₆F₃N₅O₂S

There total 5 articles about C₂₂H₁₆F₃N₅O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609271-85-3
C₂₂H₂₀BrN₅O₂S

: 1609271-86-4
C₂₂H₁₆F₃N₅O₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / water; 1,4-dioxane / 0.08 h / Microwave irradiation; Inert atmosphere

1.2: 0.33 h / 120 °C / Sealed tube; Microwave irradiation

2.1: boron tribromide / dichloromethane / 72 h / 0 - 20 °C

3.1: Dess-Martin periodane / dichloromethane / 20 °C

With boron tribromide; potassium carbonate; Dess-Martin periodane; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: 1609270-72-5
C₂₉H₂₄F₃N₅O₂S

: 1609271-86-4
C₂₂H₁₆F₃N₅O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 72 h / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 20 °C

With boron tribromide; Dess-Martin periodane; In dichloromethane;

Reference yield:

: 214360-73-3
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

: 1609271-86-4
C₂₂H₁₆F₃N₅O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h

2.1: potassium carbonate / water; 1,4-dioxane / 0.08 h / Microwave irradiation; Inert atmosphere

2.2: 0.33 h / 120 °C

3.1: potassium carbonate / water; 1,4-dioxane / 0.08 h / Microwave irradiation; Inert atmosphere

3.2: 0.33 h / 120 °C / Sealed tube; Microwave irradiation

4.1: boron tribromide / dichloromethane / 72 h / 0 - 20 °C

5.1: Dess-Martin periodane / dichloromethane / 20 °C

With boron tribromide; potassium carbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;