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Technology Process of ((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3

((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3

Base Information
  • Chemical Name:((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3
  • CAS No.:106419-06-1
  • Molecular Formula:CF3O3S*C16H38FeP3
  • Molecular Weight:528.316
  • Hs Code.:
((CH<sub>2</sub>C(CH<sub>3</sub>))2CH)Fe(P(CH<sub>3</sub>)3)3<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=((CH<sub>2</sub>C(CH<sub>3</sub>))2CH)Fe(P(CH<sub>3</sub>)3)3O<sub>3</sub>SCF<sub>3</sub>

Synonyms:((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3

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Chemical Property of ((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3
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Technology Process of ((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3

There total 1 articles about ((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

((CH<sub>2</sub>C(CH<sub>3</sub>))2CH)2Fe(P(CH<sub>3</sub>)3)
106419-01-6

((CH2C(CH3))2CH)2Fe(P(CH3)3)

trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

trimethylphosphane
594-09-2

trimethylphosphane

2,4-Dimethyl-1,3-pentadiene
1000-86-8

2,4-Dimethyl-1,3-pentadiene

{HP(CH<sub>3</sub>)3}<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup> = {HP(CH<sub>3</sub>)3}CF<sub>3</sub>SO<sub>3</sub>
106419-07-2

{HP(CH3)3}(1+)*CF3SO3(1-) = {HP(CH3)3}CF3SO3

((CH<sub>2</sub>C(CH<sub>3</sub>))2CH)Fe(P(CH<sub>3</sub>)3)3<sup>(1+)</sup>*O<sub>3</sub>SCF<sub>3</sub><sup>(1-)</sup>=((CH<sub>2</sub>C(CH<sub>3</sub>))2CH)Fe(P(CH<sub>3</sub>)3)3O<sub>3</sub>SCF<sub>3</sub>
106419-06-1

((CH2C(CH3))2CH)Fe(P(CH3)3)3(1+)*O3SCF3(1-)=((CH2C(CH3))2CH)Fe(P(CH3)3)3O3SCF3

Guidance literature:
In diethyl ether; CF3SO3H in Et2O added dropwise over 10 min to cold (-78°C), stirred soln. of Fe complex in Et2O under inert atm., stirred at -78°C for 10 min, PMe3 in Et2O added, stirred at -78°C for 45 min, allowed to warm to room temp.; mixt. of Fe complex and phosphine salt in 63:37 molar ratio pptd., detected by NMR, attempts to separate the two components were unsuccessful, elem. anal.; diene analyzed by GC;
DOI:10.1021/om00146a009
upstream raw materials:

((CH2C(CH3))2CH)2Fe(P(CH3)3)

trifluorormethanesulfonic acid

trimethylphosphane

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