(S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate

Base Information

Chemical Name:(S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate
CAS No.:1417611-80-3
Molecular Formula:C₂₉H₃₀N₂O₃
Molecular Weight:454.569
Hs Code.:

Synonyms:(S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate

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Chemical Property of (S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate

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Technology Process of (S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate

There total 2 articles about (S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₂₀H₂₂F₃N₂O₂⁽¹⁺⁾*Br^(1-)

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 1417611-80-3
(S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate

Guidance literature:: With O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; potassium hydroxide; In water; at -30 ℃; enantioselective reaction;
DOI:10.1055/s-0032-1317382

Reference yield:

: 62467-65-6
1-(6-methoxy-1H-indol-3-yl)-N,N-dimethylmethanamine

: 1417611-80-3
(S)-t-butyl 2-(diphenylmethyleneamino)-3-(6-methoxy-1H-indol-3-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 25 °C

2: potassium hydroxide; O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide / water / -30 °C

With O-allyl-N-(9-anthracenylmethyl)cinchonidinium bromide; potassium hydroxide; In dichloromethane; water;
DOI:10.1055/s-0032-1317382