5-amino-4'-[N₂,N₆-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one

Base Information

• Chemical Name: 5-amino-4'-[N₂,N₆-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one
• CAS No.: 468719-71-3
• Molecular Formula: C₃₈H₃₅F₃N₄O₇
• Molecular Weight: 716.714

Synonyms:5-amino-4'-[N₂,N₆-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one

Chemical Property of 5-amino-4'-[N₂,N₆-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one

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Technology Process of 5-amino-4'-[N₂,N₆-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one

There total 1 articles about 5-amino-4'-[N₂,N₆-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine (405-39-0) + 5-Amino-2-(4-amino-3-fluorophenyl)-6,8-difluoro-7-methyl-4H-1-benzopyran-4-one (165179-35-1) → 5-amino-4'-[N2,N6-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one (468719-71-3)

Guidance literature:

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 3 ℃; for 0.25h;

5-Amino-2-(4-amino-3-fluorophenyl)-6,8-difluoro-7-methyl-4H-1-benzopyran-4-one; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 3 - 20 ℃; for 1.75h;

Reference yield: 92.0%

5-amino-4'-[N2,N6-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one (468719-71-3) → 5-amino-6,8-difluoro-2-[3-fluoro-4-[(L-lysyl)amino]phenyl]-7-methyl-4H-1-benzopyran-4-one trihydrobromide

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 2h;

Reference yield: 90.0%

5-amino-4'-[N2,N6-(dicarbobenzyloxy)-L-lysinamido]-7-methyl-6,8,3'-trifluoro-4H-1-benzopyran-4-one (468719-71-3) → 5-amino-6,8-difluoro-2-[3-fluoro-4-[(L-lysyl)amino]phenyl]-7-methyl-4H-1-benzopyran-4-one dimethanesulfonate

Guidance literature:

With methanesulfonic acid; at 20 ℃; for 24h;

upstream raw materials:

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine

5-Amino-2-(4-amino-3-fluorophenyl)-6,8-difluoro-7-methyl-4H-1-benzopyran-4-one

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