[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄

Base Information

Chemical Name:[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄
CAS No.:882072-06-2
Molecular Formula:C₂₅H₂₂N₇O₂Ru*ClO₄
Molecular Weight:653.016
Hs Code.:

[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO<sub>4</sub>

Synonyms:[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄

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Chemical Property of [Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄

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Technology Process of [Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄

There total 1 articles about [Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: bis(acetonitrile)bis(2,4-pentanedionato)ruthenium(II)

: 3682-35-7
2,4,6-tris(2-pyridyl)-1,3,5-triazine

: sodium perchlorate

: 31378-26-4,31378-27-5,14284-93-6
tris(2,4-pentanedionato)ruthenium(III)

: 882072-06-2
[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄

Guidance literature:: In ethanol; under N2; Ru complex and ligand (molar ratio 1:1) dissolved in EtOH; heated to reflux for 10 h; solvent evapd.; dissolved in min. MeCN; aq. soln. of NaClO4 (excess) added; kept in deep freeze overnight; filtered; ppt. washed with ice-cold water and cold EtOH; dried under vac.; purified by column chromy. (neutral alumina, CH2Cl2-MeCN 20:1, 15:1);second violet band collected; solvent evapd.; elem. anal.;
DOI:10.1021/ic0514288

Reference yield: 30.0%

: 882072-06-2
[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(MeCN)]ClO₄

: 106-49-0,12221-03-3
p-toluidine

: 882072-14-2
[Ru(II)(2,4,6-tris(2-pyridyl)-1,3,5-triazine)(acetylacetonate)(H₂NC₆H₄CH₃)]ClO₄

Guidance literature:: In ethanol; under N2; Ru complex and CH3C6H4NH2 (molar ratio 1:1) dissolved in EtOH;heated to reflux for 8 h; solvent removed under reduced pressure; purified by column chromy. (neutral alumina, CH2Cl2-MeCN 3:1); solvent evapd.; elem. anal.;
DOI:10.1021/ic0514288