10-phenyl-1,2,3,4-tetrahydrophenanthrene

Base Information

Chemical Name:10-phenyl-1,2,3,4-tetrahydrophenanthrene
CAS No.:844-19-9
Molecular Formula:C₂₀H₁₈
Molecular Weight:258.363
Hs Code.:

Synonyms:10-phenyl-1,2,3,4-tetrahydrophenanthrene

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Chemical Property of 10-phenyl-1,2,3,4-tetrahydrophenanthrene

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Technology Process of 10-phenyl-1,2,3,4-tetrahydrophenanthrene

There total 6 articles about 10-phenyl-1,2,3,4-tetrahydrophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2-phenyl-2-((2',3',4',5'-tetrahydro-[1,1'-biphenyl]-2-yl)methyl)-1,3-dioxolane

: 844-19-9
10-phenyl-1,2,3,4-tetrahydrophenanthrene

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere; Reflux;
DOI:10.1021/acs.orglett.0c02020

Reference yield:

: 2-(2-bromobenzyl)-2-phenyl-1,3-dioxolane

: 844-19-9
10-phenyl-1,2,3,4-tetrahydrophenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 15 h / 100 °C / Schlenk technique; Inert atmosphere; Sealed tube

2: copper(l) chloride; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 2 h / 90 °C / Inert atmosphere; Schlenk technique; Sealed tube

3: boron trifluoride diethyl etherate / dichloromethane / 1.5 h / 0 °C / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; boron trifluoride diethyl etherate; potassium acetate; copper(l) chloride; sodium hydroxide; In 1,4-dioxane; dichloromethane; 1: |Suzuki-Miyaura Coupling / 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.orglett.0c02020

Reference yield:

: 4,4,5,5-tetramethyl-2-(2-((2-phenyl-1,3-dioxolan-2-yl)methyl)phenyl)-1,3,2-dioxaborolane

: 844-19-9
10-phenyl-1,2,3,4-tetrahydrophenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 2 h / 90 °C / Inert atmosphere; Schlenk technique; Sealed tube

2: boron trifluoride diethyl etherate / dichloromethane / 1.5 h / 0 °C / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; boron trifluoride diethyl etherate; copper(l) chloride; sodium hydroxide; In 1,4-dioxane; dichloromethane; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.orglett.0c02020