4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

Base Information

Chemical Name:4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester
CAS No.:1350441-19-8
Molecular Formula:C₂₅H₂₈F₃NO₆
Molecular Weight:495.496
Hs Code.:

Synonyms:4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

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Chemical Property of 4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

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Technology Process of 4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

There total 4 articles about 4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350441-15-4
4-ethoxycarbonylmethylaminomethylphenoxyacetic acid t-butyl ester

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 1350441-19-8
4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.25h; Cooling with ice;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1350441-19-8
4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 1 h / 60 °C

2: triethylamine; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 3 h / 20 °C

3: triethylamine / dichloromethane / 0.25 h / 20 °C / Cooling with ice

With sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; In dichloromethane; 1,2-dichloro-ethane; acetone;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1350441-19-8
4-[N-ethoxycarbonylmethyl-N-(3-trifluoromethylbenzoyl)aminomethyl]phenoxyacetic acid t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 1 h / 60 °C

2: triethylamine; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 3 h / 20 °C

3: triethylamine / dichloromethane / 0.25 h / 20 °C / Cooling with ice

With sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; In dichloromethane; 1,2-dichloro-ethane; acetone;