C₂₃H₃₃NO₄SSi

Base Information

• Chemical Name: C₂₃H₃₃NO₄SSi
• CAS No.: 1261033-73-1
• Molecular Formula: C₂₃H₃₃NO₄SSi
• Molecular Weight: 447.671
• Mol file: 1261033-73-1.mol

Synonyms:C₂₃H₃₃NO₄SSi

Chemical Property of C₂₃H₃₃NO₄SSi

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₃H₃₃NO₄SSi

There total 1 articles about C₂₃H₃₃NO₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-(4-(tert-butyldimethylsilyloxy)phenyl)propan-1-amine (522602-20-6) + 4-Acetylbenzenesulfonyl chloride (1788-10-9) → C23H33NO4SSi (1261033-73-1)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201001402

Reference yield: 95.0%

C23H33NO4SSi (1261033-73-1) → C17H19NO4S (1261033-69-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1002/chem.201001402

Reference yield:

C23H33NO4SSi (1261033-73-1) → C17H17NO4S (1261033-85-5)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere

2: [bis(acetoxy)iodo]benzene; trifluoroacetic acid / 20 °C / Inert atmosphere

With [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; trifluoroacetic acid; In tetrahydrofuran;

DOI:10.1002/chem.201001402

upstream raw materials:

3-(4-(tert-butyldimethylsilyloxy)phenyl)propan-1-amine

4-Acetylbenzenesulfonyl chloride

Downstream raw materials:

C₁₇H₁₉NO₄S

C₁₇H₁₇NO₄S