(1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

• Chemical Name: (1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
• CAS No.: 263895-04-1
• Molecular Formula: C₂₀H₂₈O₆
• Molecular Weight: 364.439

Synonyms:(1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Chemical Property of (1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Chemical Property:

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Technology Process of (1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 1 articles about (1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl chloroformate (79-22-1) + p-benzoquinone (106-51-4) + C12H21LiO2 → (1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (263895-04-1)

Guidance literature:

p-benzoquinone; C₁₂H₂₁LiO₂; In tetrahydrofuran; at -78 ℃;

methyl chloroformate; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;

DOI:10.1021/ol9913183

Reference yield: 90.0%

benzylamine (100-46-9) + (1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (263895-04-1) → Benzylamino-(4-hydroxy-phenyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ol9913183

Reference yield: 40.0%

(1-Methoxycarbonyloxy-4-oxo-cyclohexa-2,5-dienyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (263895-04-1) → Amino-(4-hydroxy-phenyl)-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:

With ammonia; In tetrahydrofuran; at -30 ℃;

DOI:10.1021/ol9913183

upstream raw materials:

methyl chloroformate

p-benzoquinone

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