Technology Process of 1-((E)-3-(2-nitrophenyl)prop-1-enyl)benzene
There total 5 articles about 1-((E)-3-(2-nitrophenyl)prop-1-enyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; silver carbonate;
In
N,N-dimethyl acetamide;
at 110 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ol5017349
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C
2: silver carbonate; 1,3-bis-(diphenylphosphino)propane; tris-(dibenzylideneacetone)dipalladium(0) / N,N-dimethyl acetamide / 12 h / 110 °C / Inert atmosphere
With
dmap; tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; dicyclohexyl-carbodiimide; silver carbonate;
In
dichloromethane; N,N-dimethyl acetamide;
1: |Steglich Esterification;
DOI:10.1021/ol5017349
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,3-bis-(diphenylphosphino)propane; tris-(dibenzylideneacetone)dipalladium(0) / N,N-dimethyl acetamide / 12 h / 160 °C
2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C
3: silver carbonate; 1,3-bis-(diphenylphosphino)propane; tris-(dibenzylideneacetone)dipalladium(0) / N,N-dimethyl acetamide / 12 h / 110 °C / Inert atmosphere
With
dmap; tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; dicyclohexyl-carbodiimide; silver carbonate;
In
dichloromethane; N,N-dimethyl acetamide;
2: |Steglich Esterification;
DOI:10.1021/ol5017349
