Technology Process of C19H29N3O2S
There total 6 articles about C19H29N3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; iron; ammonium chloride;
In
tetrahydrofuran; methanol;
for 2.5h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / diethyl ether; dimethyl sulfoxide; mineral oil / 3.58 h / 20 - 35 °C
2.1: borane-THF / tetrahydrofuran / 2.5 h / Reflux
3.1: acetone / 0.5 h / 20 °C
4.1: sodium hydroxide; water / methanol / 0.33 h / 50 °C
5.1: acetonitrile / 3 h / 50 °C
5.2: 2 h / 20 °C
6.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 2.5 h / Reflux
With
borane-THF; water; iron; sodium hydride; ammonium chloride; sodium hydroxide;
In
tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; acetone; acetonitrile; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: borane-THF / tetrahydrofuran / 2.5 h / Reflux
2.1: acetone / 0.5 h / 20 °C
3.1: sodium hydroxide; water / methanol / 0.33 h / 50 °C
4.1: acetonitrile / 3 h / 50 °C
4.2: 2 h / 20 °C
5.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 2.5 h / Reflux
With
borane-THF; water; iron; ammonium chloride; sodium hydroxide;
In
tetrahydrofuran; methanol; acetone; acetonitrile;