Technology Process of 2-
-1-propanol
There total 10 articles about 2--1-propanol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 1.5h;
Ambient temperature;
DOI:10.1248/cpb.40.1721
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 490 mg / diethyl ether / 0.5 h / Ambient temperature
2: 94.2 percent / lithium aluminum hydride / diethyl ether / 2 h / Ambient temperature
3: 88.4 percent / pyridine / 1.5 h / 70 - 80 °C
4: 66.4 percent / aluminum chloride / CCl4 / 0.5 h / 0 - 5 °C
5: 53.3 percent / silver nitrate / acetone; H2O / 3 h / Ambient temperature
6: 11.3 percent / Jones reagent / acetone / 2 h / Ambient temperature
7: 81.2 percent / Jones reagent / acetone / 2 h / Ambient temperature
8: 93.4 percent / diethyl ether / 0.5 h / Ambient temperature
9: 94.3 percent / 15percent HCl / methanol / 1 h / Heating
10: 96.8 percent / lithium aluminum hydride / tetrahydrofuran / 1.5 h / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; jones reagent; silver nitrate;
In
tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; water; acetone;
DOI:10.1248/cpb.40.1721
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 88.4 percent / pyridine / 1.5 h / 70 - 80 °C
2: 66.4 percent / aluminum chloride / CCl4 / 0.5 h / 0 - 5 °C
3: 53.3 percent / silver nitrate / acetone; H2O / 3 h / Ambient temperature
4: 11.3 percent / Jones reagent / acetone / 2 h / Ambient temperature
5: 81.2 percent / Jones reagent / acetone / 2 h / Ambient temperature
6: 93.4 percent / diethyl ether / 0.5 h / Ambient temperature
7: 94.3 percent / 15percent HCl / methanol / 1 h / Heating
8: 96.8 percent / lithium aluminum hydride / tetrahydrofuran / 1.5 h / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; jones reagent; silver nitrate;
In
tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; water; acetone;
DOI:10.1248/cpb.40.1721