1,2-bis-1-cyclohexene

Base Information

• Chemical Name: 1,2-bis-1-cyclohexene
• CAS No.: 3999-69-7
• Molecular Formula: C₈H₁₄O₂
• Molecular Weight: 142.198
• Mol file: 3999-69-7.mol

Synonyms:1,2-bis-1-cyclohexene

Chemical Property of 1,2-bis-1-cyclohexene

Chemical Property:

Purity/Quality:

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Technology Process of 1,2-bis-1-cyclohexene

There total 5 articles about 1,2-bis-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,2-bis-1-cyclohexene diformate (75676-78-7) → 1,2-bis-1-cyclohexene (3999-69-7)

Guidance literature:

With ammonia; In methanol;

DOI:10.1055/s-1980-29114

Reference yield: 69.0%

C8H12O2 (74382-45-9) → 1,2-bis-1-cyclohexene (3999-69-7)

Guidance literature:

With bis(cyclopentadienyl)titanium dichloride; zinc; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.200802621

Reference yield: 62.0%

3,4,5,6-Tetrahydrophthalic anhydride (2426-02-0) → 1,2-bis-1-cyclohexene (3999-69-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 3h;

DOI:10.1021/acsmedchemlett.7b00406

upstream raw materials:

1,2-bis-1-cyclohexene diformate

1,2-dimethyl cyclohex-1-ene-1,2-dicarboxylate

C₈H₁₂O₂

3,4,5,6-Tetrahydrophthalic anhydride

Downstream raw materials:

1,2-Bis-(brommethyl)-1-cyclohexen