Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester
CAS No.:826994-90-5
Molecular Formula:C₂₇H₃₈O₄Si
Molecular Weight:454.682
Hs Code.:

Synonyms:Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester

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Chemical Property of Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester

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Technology Process of Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester

There total 2 articles about Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 826994-89-2
(2S,3S,4R,5R)-4-bromo-2-(2-{[tert-butyl(diphenyl)silyl]oxy}ethyl)-5-methyl-5-propyltetrahydrofuran-3-yl formate

: 826994-90-5
Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; at 80 ℃; for 4h;
DOI:10.1021/ja044130+ DOI:10.1021/ja061918e

Reference yield:

: tert-butyl{2-[(2S)-5-methyl-5-propyl-2,5-dihydrofuran-2-yl]ethoxy}diphenylsilane

: 826994-90-5
Formic acid (2S,3R,5R)-2-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-5-methyl-5-propyl-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NBS / H₂O / 6 h / -5 °C

2: (TMS)3SiH; AIBN / toluene / 4 h / 80 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In water; toluene;
DOI:10.1021/ja061918e