1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

Base Information

Chemical Name:1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane
CAS No.:312329-45-6
Molecular Formula:C₄₅H₄₆O₆Si
Molecular Weight:710.942
Hs Code.:

Synonyms:1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

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Chemical Property of 1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

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Technology Process of 1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

There total 1 articles about 1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 312329-39-8
1-(trimethylsilylethynylphenyl)-3,5,7-tris(4-carboxyphenyl)adamantane

: 312329-45-6
1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

Guidance literature:: DOI:10.1021/ja025840n

Reference yield: 95.0%

: 312329-45-6
1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

: 312329-49-0
1-(ethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; at 20 ℃;
DOI:10.1016/S0040-4039(00)01187-4

Reference yield:

: 312329-45-6
1-(4-trimethylsilylethynylphenyl)-3,5,7-tris(4-carbomethoxyphenyl)adamantane

: 444085-23-8
C₁₀H₇N₂C₂C₆H₄(CH₂)6C₄(C₆H₄CO₂CH₃)3

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / n-Bu₄NF / tetrahydrofuran / 20 °C

2.1: (Me₃Si)2NLi / tetrahydrofuran; hexane / 2.5 h / -78 °C

2.2: B-methoxy-9-BBN / Pd(PPh₃)4 / tetrahydrofuran / 18 h / Heating

With tetrabutyl ammonium fluoride; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; 2.2: Suzuki-type coupling;
DOI:10.1021/ja025840n