N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide
CAS No.:1018388-22-1
Molecular Formula:C₁₇H₁₂F₁₇NO₂S
Molecular Weight:617.327
Hs Code.:

Synonyms:N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

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Chemical Property of N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

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Technology Process of N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1018388-71-0
N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methyl-N-{tert-butoxycarbonyl}benzenesulfonamide

: 1018388-22-1
N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo7026273

Reference yield: 70.0%

: 1018388-22-1
N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

: 1120367-40-9
methyl 2-O-(2'-oxymethyl-allyl)-3,4-dideoxy-6-O-triphenylmethyl-α-D-gluco-hex-3-enopyranoside

: 1120367-41-0
(2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-trityloxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol802848j

Reference yield: 69.0%

: 1018388-15-2
(Z)-2-[4'-(tetrahydropyran-2''-yloxy)but-2'-enyloxymethyl]allyl alcohol

: 1018388-22-1
N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide

: 1018388-29-8
(Z)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-N-[2'-(4''-hydroxybut-2''-enyloxymethyl)allyl]-4-methylbenzenesulfonamide

Guidance literature:: (Z)-2-[4'-(tetrahydropyran-2''-yloxy)but-2'-enyloxymethyl]allyl alcohol; N-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)-4-methylbenzenesulfonamide; With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 0.666667h;

With toluene-4-sulfonic acid; In methanol; for 15h; Further stages.;
DOI:10.1021/jo7026273