(S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

Base Information

Chemical Name:(S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid
CAS No.:1190430-52-4
Molecular Formula:C₄₀H₄₃N₃O₇
Molecular Weight:677.797
Hs Code.:

Synonyms:(S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

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Chemical Property of (S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

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Technology Process of (S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

There total 2 articles about (S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1190430-53-5
(S)-phenylmethyl 5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)-butan-amido]-4-oxo-6-phenylhexanoate

: 1190430-52-4
(S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h;
DOI:10.1021/jo901466b

Reference yield:

: 1190430-51-3
(S)-methyl 5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoate

: 1190430-52-4
(S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

Guidance literature:: With trimethyltin(IV) hydroxide; In dichloromethane; at 70 ℃; for 4.5h;
DOI:10.1021/jo901466b

Reference yield: 80.0%

: Ala-Ile-Leu-OBn trifluoroacetate

: 1190430-52-4
(S)-5-[[(S)-2-(tert-butoxycarbonylamino)]-4-oxo-4-(triphenylmethylamino)butanamido]-4-oxo-6-phenylhexanoic acid

: 1190430-55-7
(6S,9S,15S,18S,21S)-phenylmethyl 18-sec-butyl-2,2,15,23-tetramethyl-4,7,10,13,16,19-hexaoxo-6-[2-oxo-2-(triphenylmethylamino)ethyl]-9-phenylmethyl-3-oxa-5,8,14,17,20-pentaazatetracosane-21-carboxylate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jo901466b