C₂₂H₃₂O₅

Base Information

• Chemical Name: C₂₂H₃₂O₅
• CAS No.: 1385030-54-5
• Molecular Formula: C₂₂H₃₂O₅
• Molecular Weight: 376.493
• Mol file: 1385030-54-5.mol

Synonyms:C₂₂H₃₂O₅

Chemical Property of C₂₂H₃₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₂O₅

There total 3 articles about C₂₂H₃₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

C22H30O4 (1385030-53-4) → C22H32O5 (1385030-54-5) + C22H32O5 (1385030-55-6)

Guidance literature:

C₂₂H₃₀O₄; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 3h;

With sodium perborate hexahydrate; In tetrahydrofuran; water; at 20 ℃; for 2h; optical yield given as %de;

DOI:10.1039/c2ob25940k

Reference yield:

[(1R,2S,3R,5R)-2-methyl-5-(prop-1-en-2-yl)-3-(tetrahydro-2H-pyran-2-yloxy)cyclopentyl]methanol → C22H32O5 (1385030-54-5) + C22H32O5 (1385030-55-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 10 h / 20 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 0 °C

2.2: 2 h / 20 °C

With dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c2ob25940k

Reference yield:

(1R,2S,3R,5R)-5-Isopropenyl-2-methyl-3-(tetrahydro-pyran-2-yloxy)-cyclopentanecarboxylic acid methyl ester → C22H32O5 (1385030-54-5) + C22H32O5 (1385030-55-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.33 h / 20 °C

2.1: triethylamine / dichloromethane / 10 h / 20 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 0 °C

3.2: 2 h / 20 °C

With lithium aluminium tetrahydride; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c2ob25940k

upstream raw materials:

C₂₂H₃₀O₄

Downstream raw materials:

(?)-terpestacin

C₂₆H₄₀O₇