7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one

Base Information

• Chemical Name: 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one
• CAS No.: 1357572-14-5
• Molecular Formula: C₂₇H₁₈N₄O₂
• Molecular Weight: 430.466

Synonyms:7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one

Chemical Property of 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one

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Technology Process of 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one

There total 3 articles about 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C21H14N2O4 (1357571-97-1) + 1,2-diamino-benzene (95-54-5) → 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one (1357572-14-5) + C27H20N4O3 (1357572-42-9)

Guidance literature:

In acetic acid; for 2h; Reflux;

DOI:10.1002/jhet.756

Reference yield:

anthranilic acid amide (28144-70-9,88-68-6) → 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one (1357572-14-5) + C27H20N4O3 (1357572-42-9)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / benzene / Reflux

2: sodium hydroxide / water; N,N-dimethyl-formamide

With acetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; benzene;

DOI:10.1002/jhet.756

Reference yield:

2-phenyl-4-(2-furylmethylidene)-2-oxazolin-5-one (77012-48-7,15601-47-5) → 7-(2-furylmethylidene)-9-phenyl-6,7-dihydro-5H-[1,4]benzodiazepino[5,4-b][1,3,5]benzotriazepin-6-one (1357572-14-5) + C27H20N4O3 (1357572-42-9)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / benzene / Reflux

2: sodium hydroxide / water; N,N-dimethyl-formamide

With acetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; benzene;

DOI:10.1002/jhet.756

upstream raw materials:

C₂₁H₁₄N₂O₄

1,2-diamino-benzene

2-phenyl-4-(2-furylmethylidene)-2-oxazolin-5-one

anthranilic acid amide

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