4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl

Base Information

• Chemical Name: 4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl
• CAS No.: 913648-12-1
• Molecular Formula: C₆₃H₇₉ClO₄
• Molecular Weight: 935.771
• Mol file: 913648-12-1.mol

Synonyms:4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl

Chemical Property of 4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl

There total 1 articles about 4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl-4-yl]methanol (913648-10-9) → 4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl (913648-12-1)

Guidance literature:

With thionyl chloride; 2,6-di-tert-butyl-4-methylpyridine; N,N-dimethyl-formamide; In dichloromethane; at 40 ℃; for 1h;

DOI:10.1002/chem.200600178

Reference yield: 62.0%

4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl (913648-12-1) + 1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) → 3,5-bis[3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl-4-ylmethoxy]benzoic acid methyl ester

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

DOI:10.1002/chem.200601582

Reference yield: 21.8%

4-chloromethyl-3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl (913648-12-1) + methyl 3′,5′-dihydroxy-[1,1′-biphenyl]-4-carboxylate (913647-93-5) → methyl 3',5'-bis[3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl-4-ylmethoxy]biphenyl-4-carboxylate (784213-00-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 36h;

DOI:10.1002/chem.200600178

upstream raw materials:

[3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl-4-yl]methanol

Downstream raw materials:

methyl 3',5'-bis[3',4'-bis(4'-dodecyloxybiphenyl-4-ylmethoxy)biphenyl-4-ylmethoxy]biphenyl-4-carboxylate