Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

Base Information

Chemical Name:Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid
CAS No.:86823-94-1
Molecular Formula:C₁₂H₈N₂O₅
Molecular Weight:260.206
Hs Code.:

Synonyms:Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

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Chemical Property of Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

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Technology Process of Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

There total 3 articles about Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 86823-93-0
diphenylmethyl 2-[(1R,5S)-3-phenyl-7-oxo-4-oxa-2,6-diazabicyclo[3.2.0]hept-2-en-6-yl]-2-oxo acetate

: 86823-94-1
Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.333333h;

Reference yield:

: 67977-61-1,68107-98-2
epi-Secopenicillin

: 86823-94-1
Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / triethylamine / CH₂Cl₂ / 6 h / Ambient temperature

2: 1) O₃; 2) (CH₃)2S / 1) CH₂Cl₂, -70 deg C

3: 68 percent / CF₃COOH, anisole / CH₂Cl₂ / 0.33 h / 0 °C

With dimethylsulfide; ozone; methoxybenzene; triethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 68057-04-5
(1R,5S)-3-phenyl-6-(1-diphenylmethoxycarbonyl-2-methylprop-1-enyl)-7-oxo-4-oxa-2,6-diazabicyclo[3.2.0]hept-2-ene

: 86823-94-1
Oxo-((1R,5S)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) O₃; 2) (CH₃)2S / 1) CH₂Cl₂, -70 deg C

2: 68 percent / CF₃COOH, anisole / CH₂Cl₂ / 0.33 h / 0 °C

With dimethylsulfide; ozone; methoxybenzene; trifluoroacetic acid; In dichloromethane;