C₄₅H₅₉N₅O₁₁

Base Information

Chemical Name:C₄₅H₅₉N₅O₁₁
CAS No.:873676-55-2
Molecular Formula:C₄₅H₅₉N₅O₁₁
Molecular Weight:845.99
Hs Code.:

C<sub>45</sub>H<sub>59</sub>N<sub>5</sub>O<sub>11</sub>

Synonyms:C₄₅H₅₉N₅O₁₁

Suppliers and Price of C₄₅H₅₉N₅O₁₁

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₅H₅₉N₅O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₅H₅₉N₅O₁₁

There total 17 articles about C₄₅H₅₉N₅O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 166196-06-1
3-tert-butoxycarbonylamino-2-hydroxyhexanoic acid

: 873676-55-2
C₄₅H₅₉N₅O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1: 3-hydroxy-1,2,3-benzotriazin-4(3H)-one; EDC; N-methylmorpholine / dimethylformamide; CH₂Cl₂ / -20 - -10 °C

2: hydrogen / palladium on carbon / ethanol / 3 h / 20 °C

3: 3-hydroxy-1,2,3-benzotriazin-4(3H)-one; EDC; N-methylmorpholine / dimethylformamide; CH₂Cl₂ / -20 °C

4: HCl / dioxane; ethyl acetate / 0.25 h / 20 °C

5: 3-hydroxy-1,2,3-benzotriazin-4(3H)-one; EDC; N-methylmorpholine / dimethylformamide; CH₂Cl₂ / -20 - -10 °C

6: 41 mg / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; hydrogen; Dess-Martin periodane; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.200501553

Reference yield:

: 367258-43-3
(3-tert-butoxycarbonylamino-2-hydroxyhexanoylamino)acetic acid benzyl ester

: 873676-55-2
C₄₅H₅₉N₅O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / palladium on carbon / ethanol / 3 h / 20 °C

2: 3-hydroxy-1,2,3-benzotriazin-4(3H)-one; EDC; N-methylmorpholine / dimethylformamide; CH₂Cl₂ / -20 °C

3: HCl / dioxane; ethyl acetate / 0.25 h / 20 °C

4: 3-hydroxy-1,2,3-benzotriazin-4(3H)-one; EDC; N-methylmorpholine / dimethylformamide; CH₂Cl₂ / -20 - -10 °C

5: 41 mg / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; hydrogen; Dess-Martin periodane; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.200501553

Reference yield:

: 3,4-dihydroxy-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

: 873676-55-2
C₄₅H₅₉N₅O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1: magnesium sulfate; p-toluenesulfonic acid monohydrate / CH₂Cl₂ / 0 - 20 °C

2: 100 percent / HCl / dioxane / 1 h / 20 °C

3: 76 percent / HATU; ethyldiisopropylamine / CH₂Cl₂ / 18 h / 0 - 20 °C

4: 100 percent / HCl / dioxane; ethyl acetate / 20 °C

5: HATU; ethyldiisopropylamine / CH₂Cl₂ / 0 - 20 °C

6: 100 percent / hydrogen / palladium on carbon / ethyl acetate; ethanol / 16 h / 20 °C

7: 72 percent / 1,1'-(azodicarbonyl)dipiperidine; triphenylphosphane / CH₂Cl₂ / 24 h / 20 °C

8: lithium hydroxide / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

9: 3-hydroxy-1,2,3-benzotriazin-4(3H)-one; EDC; N-methylmorpholine / dimethylformamide; CH₂Cl₂ / -20 - -10 °C

10: 41 mg / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; lithium hydroxide; hydrogen; magnesium sulfate; Dess-Martin periodane; toluene-4-sulfonic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; triphenylphosphine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1,1'-azodicarbonyl-dipiperidine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; 7: Mitsunobu reaction;
DOI:10.1002/anie.200501553