tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)

Base Information

Chemical Name:tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)
CAS No.:1032103-15-3
Molecular Formula:C₁₆H₁₀Cl₂NiS₄*C₁₆H₃₆N
Molecular Weight:702.584
Hs Code.:

Synonyms:tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)

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Chemical Property of tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)

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Technology Process of tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)

There total 1 articles about tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: nickel(II) chloride hexahydrate

: 49675-82-3
4-(p-chlorophenyl)-1,3-dithiol-2-one

: 1643-19-2
tetrabutylammomium bromide

: 1032103-15-3
tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)

Guidance literature:: With Na; CH₃OH; air; In methanol; ClC6H4C3HS2O dissolved in MeOH, Na added, stirred for 10 min under N2 atroom temp., a soln. of NiCl2*6H2O added, stirred for 10 min, a soln. of N(C4H9)4Br added; washed (MeOH), dried (vac.); elem. anal.;
DOI:10.1021/ic701408m

Reference yield: 84.0%

: 1032103-15-3
tetra-n-butylammonium bis(2-(p-chlorophenyl)-1,2-dithiolato)nickelate(III)

: 1032103-29-9
bis(2-(p-chlorophenyl)-1,2-dithiolato)nickel(IV)

Guidance literature:: With I₂; In acetonitrile; I2 in MeCN added to a soln. of Ni complex, stirred for 30 min; elem. anal.;
DOI:10.1021/ic701408m