2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

Base Information

Chemical Name:2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone
CAS No.:144336-37-8
Molecular Formula:C₁₇H₂₂O₆
Molecular Weight:322.358
Hs Code.:

Synonyms:2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

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Chemical Property of 2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

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Technology Process of 2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

There total 4 articles about 2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 144336-35-6,144336-36-7
(Z)-methyl 7-O-acetyl-4,6-O-isopropylidene-7-C-phenyl-D-ido-hept-2-enoate

: 144336-37-8
2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

Guidance literature:: With potassium carbonate; In methanol; for 1h;
DOI:10.1039/P19920001907

Reference yield:

: 144336-38-9
5-O-acetyl-2,4-O-isopropylidene-5-C-phenyl-D-ido-pentose

: 144336-37-8
2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / CH₂Cl₂ / 2 h / Ambient temperature

2: 85 percent / potassium carbonate / methanol / 1 h

With potassium carbonate; In methanol; dichloromethane;
DOI:10.1039/P19920001907

Reference yield:

: 144336-34-5
1-O-acetyl-2,4-O-isopropylidene-1-C-phenyl-D-glycero-D-iodo-hexitol

: 144336-37-8
2-deoxy-4,6-O-isopropylidene-3-O-methyl-7-C-phenyl-D-glycero-L-ido-heptono-δ-lactone

Guidance literature:: Multi-step reaction with 3 steps

1: aq. sodium metaperiodate / methanol / 1 h / Ambient temperature

2: 76 percent / CH₂Cl₂ / 2 h / Ambient temperature

3: 85 percent / potassium carbonate / methanol / 1 h

With sodium periodate; potassium carbonate; In methanol; dichloromethane;
DOI:10.1039/P19920001907