3,5-difluorophenylboric acid

Base Information

Chemical Name:3,5-difluorophenylboric acid
CAS No.:147437-97-6
Molecular Formula:C₆H₅BF₂O₃
Molecular Weight:173.912
Hs Code.:

Synonyms:3,5-difluorophenylboric acid

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Chemical Property of 3,5-difluorophenylboric acid

Chemical Property:

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Technology Process of 3,5-difluorophenylboric acid

There total 1 articles about 3,5-difluorophenylboric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5419-55-6
Triisopropyl borate

: 461-96-1
3,5-difluorobromobenzene

: 147437-97-6
3,5-difluorophenylboric acid

Guidance literature:: With hydrogenchloride; n-butyllithium; In tetrahydrofuran; hexane;

Reference yield:

: 147437-97-6
3,5-difluorophenylboric acid

: 589-87-7
1,4-bromoiodobenzene

: 4-bromo-3',5'-difluorobiphenyl

Guidance literature:: With potassium carbonate; palladium-carbon; In ethanol; water; toluene;

Reference yield:

: 147437-97-6
3,5-difluorophenylboric acid

: 1353578-22-9
C₃₃H₂₄F₁₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: bis(triphenylphosphine)palladium(II) dichloride; triphenylphosphine; potassium carbonate; tetrabutylammomium bromide / ethanol; toluene / 6 h / 80 °C / Inert atmosphere

2.1: magnesium / tetrahydrofuran / 20 - 30 °C / Inert atmosphere

2.2: 6 h / 50 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

4.1: potassium carbonate; tetrabutylammomium bromide / ethanol; toluene; water / 3 h / 70 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -40 °C / Inert atmosphere

5.2: 0.5 h / 40 °C / Inert atmosphere

5.3: 5 h / 80 °C / Inert atmosphere

With n-butyllithium; bis(triphenylphosphine)palladium(II) dichloride; tetrabutylammomium bromide; potassium carbonate; magnesium; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; water; toluene;