C₁₂H₁₂F₃N₃S

Base Information

Chemical Name:C₁₂H₁₂F₃N₃S
CAS No.:1311387-63-9
Molecular Formula:C₁₂H₁₂F₃N₃S
Molecular Weight:287.309
Hs Code.:

C<sub>12</sub>H<sub>12</sub>F<sub>3</sub>N<sub>3</sub>S

Synonyms:C₁₂H₁₂F₃N₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₂F₃N₃S

Chemical Property:

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Technology Process of C₁₂H₁₂F₃N₃S

There total 5 articles about C₁₂H₁₂F₃N₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311387-98-0
C₂₂H₂₈F₃N₃O₄S

: 1311387-63-9
C₁₂H₁₂F₃N₃S

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 532-55-8
Benzoyl isothiocyanate

: 1311387-63-9
C₁₂H₁₂F₃N₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: acetone / 0.5 h / 0 °C

1.2: 40 °C

2.1: tetrahydrofuran / 6 h / 20 - 60 °C

3.1: ammonium chloride; iron / water; tetrahydrofuran; methanol / 5 h / 60 °C

4.1: dichloromethane / 4 h / 20 - 40 °C

5.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

5.2: 1 h / -78 °C

6.1: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 0 - 20 °C

7.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diethylamino-sulfur trifluoride; iron; ammonium chloride; trifluoroacetic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; water; acetone;

Reference yield:

: 1311387-88-8
C₁₆H₂₀FN₃O₂S

: 1311387-63-9
C₁₂H₁₂F₃N₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 4 h / 20 - 40 °C

2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: 1 h / -78 °C

3.1: diethylamino-sulfur trifluoride / dichloromethane / 8 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diethylamino-sulfur trifluoride; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane;