3-amino-1-butan-2-one oxime

Base Information

• Chemical Name: 3-amino-1-butan-2-one oxime
• CAS No.: 770677-71-9
• Molecular Formula: C₁₂H₁₉N₃O₂
• Molecular Weight: 237.302

Synonyms:3-amino-1-butan-2-one oxime

Chemical Property of 3-amino-1-butan-2-one oxime

Chemical Property:

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Technology Process of 3-amino-1-butan-2-one oxime

There total 1 articles about 3-amino-1-butan-2-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-{2-[(E)-Hydroxyimino]-3-[(4-methoxy-phenyl)-methyl-amino]-1-methyl-propyl}-isoindole-1,3-dione (135696-66-1) → 3-amino-1-butan-2-one oxime (770677-71-9)

Guidance literature:

With hydrazine; In ethanol; at 45 ℃; for 16h;

DOI:10.1021/jm00115a005

Reference yield: 93.0%

3-amino-1-butan-2-one oxime (770677-71-9) + ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate (6506-86-1) → (6-Amino-4-{2-[(E)-hydroxyimino]-3-[(4-methoxy-phenyl)-methyl-amino]-1-methyl-propylamino}-5-nitro-pyridin-2-yl)-carbamic acid ethyl ester (105782-26-1)

Guidance literature:

With triethylamine; In ethanol; for 16h; Heating;

DOI:10.1021/jm00115a005

Reference yield:

3-amino-1-butan-2-one oxime (770677-71-9) → Ethyl 5-amino-1,2-dihydro-3-[[N-(4-methoxyphenyl)-N-methylamino]methyl]-2-methylpyrido[3,4-b]pyrazine-7-carbamate (87607-27-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / triethylamine / ethanol / 16 h / Heating

2: 31 percent / H₂ / Raney Ni / ethanol / 66 h / 760 Torr

With hydrogen; triethylamine; nickel; In ethanol;

DOI:10.1021/jm00115a005

upstream raw materials:

2-{2-[(E)-Hydroxyimino]-3-[(4-methoxy-phenyl)-methyl-amino]-1-methyl-propyl}-isoindole-1,3-dione

Downstream raw materials:

(6-Amino-4-{2-[(E)-hydroxyimino]-3-[(4-methoxy-phenyl)-methyl-amino]-1-methyl-propylamino}-5-nitro-pyridin-2-yl)-carbamic acid ethyl ester

Ethyl 5-amino-1,2-dihydro-3-[[N-(4-methoxyphenyl)-N-methylamino]methyl]-2-methylpyrido[3,4-b]pyrazine-7-carbamate

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