(+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

Base Information

Chemical Name:(+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate
CAS No.:77029-34-6
Molecular Formula:C₄₀H₄₀As₄ClPd*Cl*2H₂O
Molecular Weight:1033.8
Hs Code.:

Synonyms:(+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

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Chemical Property of (+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

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Technology Process of (+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

There total 1 articles about (+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 52120-04-4,55289-90-2,55289-91-3,57341-01-2,57375-33-4
(RR)-o-phenylenebis(methylphenylarsine)

: 73089-28-8,57385-76-9,57385-77-0,73089-27-7
[PdCl₂((SS)-o-phenylenebis(methylphenylarsine))]

: 77029-34-6
(+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

Guidance literature:: In ethanol; mixt. (PdCl2((SS)-diars)) and (RR)-diars in ethanol heated until solidsdissolved; soln. filtered and filtrate diluted with diethyl ether; elem. anal.;

Reference yield: 71.0%

: ammonium hexafluorophosphate

: 77029-34-6
(+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

: 77059-83-7
(+)589-bis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) hexafluorophosphate

Guidance literature:: In water; soln. optically active chloride in boiling water treated with NH4PF6 inwater; ppt. filtered off, washed with water, dried and recrystd. from hot methanol; elem. anal.;

Reference yield: 68.0%

: 77029-34-6
(+)589-chlorobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) chloride dihydrate

: 77029-35-7
(+)589-iodobis((SS)-o-phenylenebis(methylphenylarsine))palladium(II) iodide

Guidance literature:: With sodium iodide; In water; NaI added to soln. corresponding chloride in hot water; ppt. recrystd. from dichloromethane-diethyl ether; elem. anal.;